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Simultaneous Electrochemical Detection of Ascorbic Acid, Dopamine and Uric Acid Using the Composite Materials of Fe₃O₄ and Nitrogen Self-Doped Sunflower Plate-Derived Carbon

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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Yaqi Huang

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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Yaoyao Zhang

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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Qiaoqian Sun

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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Shaojie Ruan

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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Wei Yin

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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Hongchen Pu

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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Miao Yin

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

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, and

Huanbao Fa

https://orcid.org/0000-0001-7456-9679

National-Municipal Joint Engineering Laboratory for Chemical Process, Intensification and Reaction, School of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, P. R. China

E-mail Address: [email protected]

Corresponding author.

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https://doi.org/10.1142/S1793292021501277Cited by:2 (Source: Crossref)

Abstract

A simple pyrolysis, activation and hydrothermal method was utilized to synthesize composite materials (Fe₃O₄/SFP) of ferroferric oxide and nitrogen self-doped sunflower plate-derived carbon for the simultaneous electrochemical sensing of ascorbic acid (AA), dopamine (DA) and uric acid (UA). The Fe₃O₄/SFP had synergistic catalytic effect on target molecules, and the oxidation peak potential of AA, DA and UA was well distinguished in the differential pulse voltammetry determination. Under the optimal conditions, the linear response ranges of AA, DA and UA are 3–150 $μ$ M, 5–450 $μ$ M and 15–1200 $μ$ M, respectively. The detection limits of AA, DA and UA ( $S$ / $N = 3$ ) are 1.0 $μ$ M, 0.4 $μ$ M and 1.48 $μ$ M, respectively, and the sensitivity is 1.87 $μ A \cdot μ M^{- 1} \cdot {cm}^{- 2}$ (3–20 $μ$ M) and 0.64 $μ A \cdot μ M^{- 1} \cdot {cm}^{- 2}$ (20–150 $μ$ M) for AA, 3.90 $μ A \cdot μ M^{- 1} \cdot {cm}^{- 2}$ (5–20 $μ$ M) and 1.21 $μ A \cdot μ M^{- 1} \cdot {cm}^{- 2}$ (20–450 $μ$ M) for DA and 1.12 $μ A \cdot μ M^{- 1} \cdot {cm}^{- 2}$ (15–100 $μ$ M) and 0.31 $μ A \cdot μ M^{- 1} \cdot {cm}^{- 2}$ (100–1200 $μ$ M) for UA. In addition, satisfactory results have been obtained for the determination of AA, DA and UA in normal human serum, which provides a new research direction for the construction of electrochemical sensors in the future.

Keywords:

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Vol. 16, No. 11

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History

Received 26 March 2021

Accepted 16 August 2021

Published: 30 September 2021

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Simultaneous Electrochemical Detection of Ascorbic Acid, Dopamine and Uric Acid Using the Composite Materials of Fe₃O₄ and Nitrogen Self-Doped Sunflower Plate-Derived Carbon

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Simultaneous Electrochemical Detection of Ascorbic Acid, Dopamine and Uric Acid Using the Composite Materials of Fe3O4 and Nitrogen Self-Doped Sunflower Plate-Derived Carbon

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