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Pd-Decorated NiCo₂O₄ Nanotubes Derived from Template-Free Process for Improved Electrocatalytic Glucose Oxidation

Heyu Zhao

College of Materials & Environmental Engineering, Hangzhou Dianzi University, Hangzhou 310018, P. R. China

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Haoyong Yin

https://orcid.org/0000-0002-1628-308X

College of Materials & Environmental Engineering, Hangzhou Dianzi University, Hangzhou 310018, P. R. China

E-mail Address: yhy@hdu.edu.cn

Corresponding authors.

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Ling Wang

Department of Chemistry, Zhejiang Sci-Tech University, Hangzhou 310018, P. R. China

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Yifan Zheng

Research Center of Analysis and Measurement, Zhejiang University of Technology, Hangzhou 310014, P. R. China

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Shumin Zhao

College of Materials & Environmental Engineering, Hangzhou Dianzi University, Hangzhou 310018, P. R. China

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, and

Shengji Wu

College of Engineering, Huzhou University, Huzhou 313000, P. R. China

E-mail Address: wushengji26@hdu.edu.cn

Corresponding authors.

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https://doi.org/10.1142/S1793292022500710Cited by:0 (Source: Crossref)

Abstract

The electrode materials for highly efficient glucose oxidation reaction (GOR) are vital for nonenzymatic glucose sensors (NEGS) and direct glucose fuel cells. The Pd-decorated NiCo₂O₄ nanotubes (Pd/NiCo₂O₄ NTs) were prepared through the template-free process. Pd/NiCo₂O₄ NTs presented highly improved electrocatalytic activity for glucose oxidation. When applied to glucose detection, Pd/NiCo₂O₄ NTs displayed superior sensing performance with a wide detection range of 5 $μ$ M–9 mM. The sensitivity and detection limit are 214.2 $μ A \cdot {mM}^{- 1} \cdot {cm}^{- 2}$ and 1.6 $μ$ M, respectively. Moreover, the Pd/NiCo₂O₄ NTs sensors also demonstrated excellent selectivity and feasibility for glucose detection for serum sample analysis.

Keywords:

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