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    Sintering and kinetic mechanism of Si3N4-SiC micro-nano composite by spark plasma sintering

    Si3N4–SiC composites were fabricated by spark plasma sintering at 1700C for 480 S with MgSiN2 and Y2O3 as additives. The morphology and phase characterization of the composites were characterized using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The values of n parameter indicate that the grain boundary reaction is the rate controller at 1500C and diffusion becomes the controlling step at 1550C. The nanohardness and Young’s modulus attained the maximum value of 18.5 and 316GPa, respectively.