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Synthesis of Trilaminar Core–Shell Au/ $α$ -Fe₂O₃@SnO₂Nanocomposites and their Application for Nonenzymatic Dopamine Electrochemical Sensing

Key Laboratory of Shaanxi Administration of Traditional Chinese Medicine for TCM Compatibility, and Shaanxi Key Laboratory of Chinese Medicine Fundamentals and New Drugs Research and Shaanxi Collaborative Innovation, Center of Chinese Medicinal Resources Industrialization, Shaanxi University of Chinese Medicine, Xi’an 712046, P. R. China

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Shijun Yue

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Jiajia Li

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Jianbin Zheng

College of Chemistry & Materials Science/Shaanxi, Provincial Key Laboratory of Electroanalytical Chemistry, Northwest University, Xi’an, Shaanxi 710069, P. R. China

E-mail Address: zhengjb@nwu.edu.cn

Corresponding author.

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, and

Guojie Gao

China National Heavy Machinery Research Institute Co., Ltd., P. R. China

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https://doi.org/10.1142/S1793292019501388Cited by:3 (Source: Crossref)

Abstract

Au nanoparticles anchored on core–shell $α$ -Fe₂O₃@SnO₂ nanospindles were successfully constructed through hydrothermal synthesis process and used for fabricating a novel nonenzymatic dopamine (DA) sensor. The structure and morphology of the Au/ $α$ -Fe₂O₃@SnO₂ trilaminar nanohybrid film were characterized by scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The electrochemical properties of the sensor were investigated by cyclic voltammetry and amperometry. The experimental results suggest that the composites have excellent catalytic property toward DA with a wide linear range from 0.5 $μ$ M to 0.47mM, a low detection limit of 0.17 $μ$ M (S/ $N = 3$ ) and high sensitivity of 397.1 $μ$ AmM $^{- 1}$ cm $^{- 2}$ . In addition, the sensor exhibits long-term stability, good reproducibility and anti-interference.

Keywords:

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Vol. 14, No. 11

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History

Received 27 June 2019

Accepted 11 September 2019

Published: 6 November 2019

Keywords

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System Upgrade on Tue, May 28th, 2024 at 2am (EDT)

Synthesis of Trilaminar Core–Shell Au/ $α$ -Fe₂O₃@SnO₂Nanocomposites and their Application for Nonenzymatic Dopamine Electrochemical Sensing

Abstract

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