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In this study, the heat-damage process of a carbon fiber reinforced plastic (CFRP) under monotonic tensile loading was characterized by acoustic emission. Additionally, epoxy specimens and prepreg specimens were used to determine the characteristics of acoustic emission (AE) signals of epoxy and fiber, respectively. The AE characteristics of CFRP showed three types of distinct frequency regions. Time-frequency analysis methods were employed for the analysis of fracture mechanisms in CFRP such as matrix cracking, debonding and fiber fracture. To evaluate the cumulative counts of AE signals, it seems that the results can be applied usefully to guarantee structural integrity and/or to the survey of destruction of the structure with heat-damage, that was made to the composite materials.
Objective: To compare the fracture mode of lithium disilicate ceramics and zirconia ceramics through a single-load-to-failure test, and reveal the cause of failure through the fractographic analysis of fracture morphology. Methods: Based on the standardized preparations, 10 IPS e.max disilicate ceramic crowns (IPCs) and 10 monolithic zirconia ceramic crowns (MZCs) were designed and fabricated. All the specimens were placed on a universal material testing machine for a single-load-to-failure test. The fracture load was recorded, and two independent sample t-tests were performed. Additionally, the type of fracture under a stereo-microscope was observed, and the morphological characteristics of the fracture with a scanning electron microscope (SEM) were investigated. Results: The fracture load of the IPC group was 1819.29±108.13N, and that of the MZC group was 4347.41±739.90N, with a statistically significant difference (t=−10.69, p<0.001). The fracture types of the IPC group and the MZC group were similar, namely, types II and III. The fracture modes of the two groups were all ceramic layer fracture. Through SEM, the origin of the crack on the occlusal surface could be traced back. The crystal fracture of IPC group had a rock sugar-like pattern, and the crystal distribution of MZC group was uniform. Conclusions: Zirconia ceramics have higher fracture load and a denser crystal structure compared to lithium disilicate. Fractographic analysis method could be a better way to analyze the failure mode of single-layer porcelain materials and reveal the origin of fracture.
In this study Al2O3-SiC nanocomposites have been fabricated by mixing of alumina and silicon carbide nano powders, followed by hot pressing at 1700°C. The mechanical properties and fracture mode of Al2O3-SiC nanocomposites containing different volume fractions (5, 10 and 15%) of nano scale SiC particles were investigated and compared with those of alumina. Al2O3-SiC powders were prepared by planetary milling in isopropanol. Fracture mode of specimens was investigated by means of scanning electron microscopy. Nanocomposites were tougher than alumina when they were hot pressed at the same temperature, and the values of nanocomposite's flexural strength and hardness were higher than those of alumina. Flexural strength, hardness and fracture toughness of the nanocomposites increase by increasing the volume percent of SiC up to 10% and then decrease slightly. The Scanning electron microscopy observations showed that fracture mode changes from intergranular for alumina to transgranular for nanocomposites. Finally X-ray diffraction analysis couldn't detect any chemical reactions between Al2O3 and SiC particles.
In this paper, the spot welding technology of 22MnMoB hot stamping quenched steel was systematically studied. Through a series of experiments, the optimal spot welding technological parameter has been obtained. The interfacial fracture tendency of spot welds of hot stamping quenched steel behavior was more obvious than that of mild steel. The test results showed that the traditional prediction equation of critical nugget diameter for the changing of fracture mode was not in accordance with test results. A new kind of sphere model which considering the structural complexity of spot weld of hot stamping quenched steel was created to obtain the critical fracture diameter value. The fracture test results of five kinds of hot stamping quenched steel showed that the model has a perfect accuracy which is more accurate and helpful to actual engineering.