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Spark plasma sintering (SPS) of pure commercially sub-micron B4C powder at 1700–1900∘C for 20min has been conducted and their wear properties have been investigated by reciprocating friction and wear test. It was found that the relative density increased with the increase and the grain size increased a little at 1700–1900∘C. Wear mechanisms in the temperature range of 1700–1900∘C have been proposed such that at 1700∘C the wear mechanism was dominated by plastic deformation and intergranular fracture, while at 1800–1900∘C there was transition to the surface fracture or grain pull-out. A model for the spherical abrasive wear was proposed to describe the friction and wear of the B4C ceramics which is well-fitting with the experimental results.
Bi2O3 nanomaterials with a diversity of morphologies, such as nanoparticles, nanorods and nanoplates, were controllably synthesized successfully by a reverse microemulsion route. X-ray diffraction (XRD), field-emission scanning electron microscope (FE-SEM), and thermogravimetry differential thermal analysis (TG-DTA) were employed to characterize the obtained products. It was found that the size and morphology of bismuth oxide were affected mainly by water content (W0), and the shape of Bi2O3 changed with different W0. The common role of surfactant adsorbing on the surface of the nanoparticles led to the formation of Bi2O3 nanomaterials with specific morphologies. The possible formation mechanisms of these nanostructures were also discussed. With calcination temperature increasing from 275 °C to 350°C, β-Bi2O3 has transformed into α-Bi2O3 completely.
Buton rock asphalt (BRA) is usually used as modifier applied to bitumen and bituminous mixture. In this paper, the performance of hot in-plant recycling mixture modified by buton rock asphalt are evaluated using rutting test, immersion Marshall test and freeze-thaw split test. The modification mechanisms of buton rock asphalt are studied by element analysis, scanning electron microscope analysis and infrared spectrum analysis. The test results showed that buton rock asphalt could improve the rutting resistance and the ability to anti-water damage of hot in-plant recycling mixture. The combined actions of rock asphalt and RAP asphalt lead to the improvement of high-temperature stability. The high-temperature softening and miscellaneous clusters adsorption of buton rock asphalt reinforce the bonding of asphalt and aggregate, and the rock asphalt powder absorbs asphalt to increase binder viscosity and reduce flow ability, thus improving the moisture susceptibility of asphalt mixture.